Green synthesis of salicylaldehyde derivative schiff base metal complexes using microwave irradiation: Characterisation & antimicrobial studies

Green synthesis of salicylaldehyde derivative schiff base metal complexes using microwave irradiation: Characterisation & antimicrobial studies

Three series of salphen derivatives were synthesised and underwent complexation with Cd(II) ion using microwave irradiation. The synthesised compounds were characterised using FT-IR, NMR, elemental analysis, and X-ray crystallography. The FT-IR and 1H-NMR spectroscopies revealed the shifting of azom...

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Published in:Malaysian Journal of Chemistry
Main Author: 2-s2.0-85094946439
Format: Article
Language:English
Published: Malaysian Institute of Chemistry 2020
Online Access:https://www.scopus.com/inward/record.uri?eid=2-s2.0-85094946439&partnerID=40&md5=07e87466be5442cb9fb7cc7fc43c77ef
id Kassim K.; Hamali M.A.; Hussain N.H.
spelling Kassim K.; Hamali M.A.; Hussain N.H.
2-s2.0-85094946439
Green synthesis of salicylaldehyde derivative schiff base metal complexes using microwave irradiation: Characterisation & antimicrobial studies
2020
Malaysian Journal of Chemistry
22
3

https://www.scopus.com/inward/record.uri?eid=2-s2.0-85094946439&partnerID=40&md5=07e87466be5442cb9fb7cc7fc43c77ef
Three series of salphen derivatives were synthesised and underwent complexation with Cd(II) ion using microwave irradiation. The synthesised compounds were characterised using FT-IR, NMR, elemental analysis, and X-ray crystallography. The FT-IR and 1H-NMR spectroscopies revealed the shifting of azomethine peaks, as well as the disappearance of hydroxyl functional groups in ligands upon complexation, suggesting the metal bonded with the ligands in a N2O2 coordination manner. The synthesised compounds were tested for antimicrobial activities against selected bacterial strains and the results showed moderate to good activity in Cd(II) complexes containing electron donating groups compared to their respective free ligands. © 2020 Malaysian Institute of Chemistry. All rights reserved.
Malaysian Institute of Chemistry
15112292
English
Article
author 2-s2.0-85094946439
spellingShingle 2-s2.0-85094946439
Green synthesis of salicylaldehyde derivative schiff base metal complexes using microwave irradiation: Characterisation & antimicrobial studies
author_facet 2-s2.0-85094946439
author_sort 2-s2.0-85094946439
title Green synthesis of salicylaldehyde derivative schiff base metal complexes using microwave irradiation: Characterisation & antimicrobial studies
title_short Green synthesis of salicylaldehyde derivative schiff base metal complexes using microwave irradiation: Characterisation & antimicrobial studies
title_full Green synthesis of salicylaldehyde derivative schiff base metal complexes using microwave irradiation: Characterisation & antimicrobial studies
title_fullStr Green synthesis of salicylaldehyde derivative schiff base metal complexes using microwave irradiation: Characterisation & antimicrobial studies
title_full_unstemmed Green synthesis of salicylaldehyde derivative schiff base metal complexes using microwave irradiation: Characterisation & antimicrobial studies
title_sort Green synthesis of salicylaldehyde derivative schiff base metal complexes using microwave irradiation: Characterisation & antimicrobial studies
publishDate 2020
container_title Malaysian Journal of Chemistry
container_volume 22
container_issue 3
doi_str_mv
url https://www.scopus.com/inward/record.uri?eid=2-s2.0-85094946439&partnerID=40&md5=07e87466be5442cb9fb7cc7fc43c77ef
description Three series of salphen derivatives were synthesised and underwent complexation with Cd(II) ion using microwave irradiation. The synthesised compounds were characterised using FT-IR, NMR, elemental analysis, and X-ray crystallography. The FT-IR and 1H-NMR spectroscopies revealed the shifting of azomethine peaks, as well as the disappearance of hydroxyl functional groups in ligands upon complexation, suggesting the metal bonded with the ligands in a N2O2 coordination manner. The synthesised compounds were tested for antimicrobial activities against selected bacterial strains and the results showed moderate to good activity in Cd(II) complexes containing electron donating groups compared to their respective free ligands. © 2020 Malaysian Institute of Chemistry. All rights reserved.
publisher Malaysian Institute of Chemistry
issn 15112292
language English
format Article
accesstype
record_format scopus
collection Scopus
_version_ 1828987872572604416

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