Purification on kappa carrageenan by re-precipitation technique

Purification on kappa (ƙ) carrageenan was performed by dissolving ƙ-carrageenan powder in distilled water and re-precipitated in a polar solvent (ethanol) and non-polar solvent (n-hexane) separately during re-precipitation process. The purified kappa carrageenan was analyzed by using Fourier transfo...

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Bibliographic Details
Published in:Solid State Phenomena
Main Author: 2-s2.0-85120534742
Format: Conference paper
Language:English
Published: Trans Tech Publications Ltd 2021
Online Access:https://www.scopus.com/inward/record.uri?eid=2-s2.0-85120534742&doi=10.4028%2fwww.scientific.net%2fSSP.317.327&partnerID=40&md5=ce4682a4a6b66039c44cbc1624066259
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Summary:Purification on kappa (ƙ) carrageenan was performed by dissolving ƙ-carrageenan powder in distilled water and re-precipitated in a polar solvent (ethanol) and non-polar solvent (n-hexane) separately during re-precipitation process. The purified kappa carrageenan was analyzed by using Fourier transform infrared (FTIR) spectroscopy and carbon, hydrogen, nitrogen, and sulfur (CHNS) elemental analysis. The outcomes from FTIR showed there are physical changes due to intermolecular interactions which lead to decrease and lower intensity of hydroxyl band at 3345 cm-1 after re-precipitated with n-hexane, compared to re-precipitation with ethanol and unpurified ƙ-carrageenan. There were variations observed in the percentages of C, H and S in the CHNS analysis between unpurified and purified ƙ-carrageenan. The successfully purified ƙ-carrageenan are suitable to be used for further application. © 2021 Trans Tech Publications Ltd, Switzerland.
ISSN:10120394
DOI:10.4028/www.scientific.net/SSP.317.327