Synthesis route towards fine and monodisperse Ni nanoparticles via hot-injection approach
Manipulation of adding sequences have been found to influence the reaction rate, thus made it easier to produced controllable Ni nanoparticles. Hot-injection approach shown capability to significantly reduce the production time of Ni nanoparticles compared to the conventional one-pot synthesis. With...
| 發表在: | Applied Mechanics and Materials |
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| 主要作者: | |
| 格式: | Conference paper |
| 語言: | English |
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2013
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| 在線閱讀: | https://www.scopus.com/inward/record.uri?eid=2-s2.0-84886256454&doi=10.4028%2fwww.scientific.net%2fAMM.393.146&partnerID=40&md5=6066a037596d23633ceb1ed8ee4f882e |
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Nik Roselina N.R.; Azizan A.; Mei Hyie K.; Mardziah C.M.; Kasolang S.; Alias S.K.; Salleh Z. |
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Nik Roselina N.R.; Azizan A.; Mei Hyie K.; Mardziah C.M.; Kasolang S.; Alias S.K.; Salleh Z. 2-s2.0-84886256454 Synthesis route towards fine and monodisperse Ni nanoparticles via hot-injection approach 2013 Applied Mechanics and Materials 393 10.4028/www.scientific.net/AMM.393.146 https://www.scopus.com/inward/record.uri?eid=2-s2.0-84886256454&doi=10.4028%2fwww.scientific.net%2fAMM.393.146&partnerID=40&md5=6066a037596d23633ceb1ed8ee4f882e Manipulation of adding sequences have been found to influence the reaction rate, thus made it easier to produced controllable Ni nanoparticles. Hot-injection approach shown capability to significantly reduce the production time of Ni nanoparticles compared to the conventional one-pot synthesis. With minor modification on conventional polyol method, narrow, monodispersed and highly yield spherical nickel (Ni) nanoparticles were successfully produced at synthesis temperature of 60°C. Three mixing methods were investigated to study its efficiency towards producing rapid and narrower size distribution of Ni nanoparticles. Reduction processes were proposed each of the method. As-synthesized Ni nanoparticles were characterized with Transmission Electron Microscopy (TEM), Scanning Transmission Electron Microscopy (STEM) and Fourier transform infrared spectroscopy (FTIR) to analyze the size, morphology and interaction of reactants. Fine particles size distribution revealed that when hydrazine was first heated, reaction rate improved tremendously. © (2013) Trans Tech Publications, Switzerland. 16627482 English Conference paper |
| author |
2-s2.0-84886256454 |
| spellingShingle |
2-s2.0-84886256454 Synthesis route towards fine and monodisperse Ni nanoparticles via hot-injection approach |
| author_facet |
2-s2.0-84886256454 |
| author_sort |
2-s2.0-84886256454 |
| title |
Synthesis route towards fine and monodisperse Ni nanoparticles via hot-injection approach |
| title_short |
Synthesis route towards fine and monodisperse Ni nanoparticles via hot-injection approach |
| title_full |
Synthesis route towards fine and monodisperse Ni nanoparticles via hot-injection approach |
| title_fullStr |
Synthesis route towards fine and monodisperse Ni nanoparticles via hot-injection approach |
| title_full_unstemmed |
Synthesis route towards fine and monodisperse Ni nanoparticles via hot-injection approach |
| title_sort |
Synthesis route towards fine and monodisperse Ni nanoparticles via hot-injection approach |
| publishDate |
2013 |
| container_title |
Applied Mechanics and Materials |
| container_volume |
393 |
| container_issue |
|
| doi_str_mv |
10.4028/www.scientific.net/AMM.393.146 |
| url |
https://www.scopus.com/inward/record.uri?eid=2-s2.0-84886256454&doi=10.4028%2fwww.scientific.net%2fAMM.393.146&partnerID=40&md5=6066a037596d23633ceb1ed8ee4f882e |
| description |
Manipulation of adding sequences have been found to influence the reaction rate, thus made it easier to produced controllable Ni nanoparticles. Hot-injection approach shown capability to significantly reduce the production time of Ni nanoparticles compared to the conventional one-pot synthesis. With minor modification on conventional polyol method, narrow, monodispersed and highly yield spherical nickel (Ni) nanoparticles were successfully produced at synthesis temperature of 60°C. Three mixing methods were investigated to study its efficiency towards producing rapid and narrower size distribution of Ni nanoparticles. Reduction processes were proposed each of the method. As-synthesized Ni nanoparticles were characterized with Transmission Electron Microscopy (TEM), Scanning Transmission Electron Microscopy (STEM) and Fourier transform infrared spectroscopy (FTIR) to analyze the size, morphology and interaction of reactants. Fine particles size distribution revealed that when hydrazine was first heated, reaction rate improved tremendously. © (2013) Trans Tech Publications, Switzerland. |
| publisher |
|
| issn |
16627482 |
| language |
English |
| format |
Conference paper |
| accesstype |
|
| record_format |
scopus |
| collection |
Scopus |
| _version_ |
1828987882883252224 |