Recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions

Over the years, recent advancements have provided new insights into the functionalisation and synthesis of graphene oxide-based materials for sample preparation applications, utilising deep eutectic solvents (DESs). The demand for efficient, selective, innovative, and simple sample preparation of co...

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Published in:Microchemical Journal
Main Author: Emmanuel Ibukun A.; Yahaya N.; Husaini Mohamed A.; Semail N.-F.; Abd Hamid M.A.; Nadhirah Mohamad Zain N.; Anuar Kamaruddin M.; Hong Loh S.; Kamaruzaman S.
Format: Review
Language:English
Published: Elsevier Inc. 2024
Online Access:https://www.scopus.com/inward/record.uri?eid=2-s2.0-85184484059&doi=10.1016%2fj.microc.2024.110111&partnerID=40&md5=4955a88ecd5bbafa5917f01555da639e
id 2-s2.0-85184484059
spelling 2-s2.0-85184484059
Emmanuel Ibukun A.; Yahaya N.; Husaini Mohamed A.; Semail N.-F.; Abd Hamid M.A.; Nadhirah Mohamad Zain N.; Anuar Kamaruddin M.; Hong Loh S.; Kamaruzaman S.
Recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions
2024
Microchemical Journal
199

10.1016/j.microc.2024.110111
https://www.scopus.com/inward/record.uri?eid=2-s2.0-85184484059&doi=10.1016%2fj.microc.2024.110111&partnerID=40&md5=4955a88ecd5bbafa5917f01555da639e
Over the years, recent advancements have provided new insights into the functionalisation and synthesis of graphene oxide-based materials for sample preparation applications, utilising deep eutectic solvents (DESs). The demand for efficient, selective, innovative, and simple sample preparation of contaminants and pollutants from various matrices has rapidly focused on dispersive and magnetic solid-phase extraction. This study summarises the use of graphene oxide and reduced graphene materials in DES-based synthesis and functionalisation, along with their physicochemical characteristics and applications in dispersive and magnetic solid-phase extraction. The majority of DESs have demonstrated significant enhancements in the extraction of targeted analytes by increasing the effective surface area for active sites and introducing desired functionalities. Upon reviewing the existing literature, it was observed that DESs were functionalised either during or after the production of graphene materials. The findings highlight that dispersive and magnetic solid-phase extraction, incorporated with DES-functionalised graphene adsorbents, offer superior advantages for routine sample pretreatment of analytes, leading to enhanced analytical performance. © 2024 Elsevier B.V.
Elsevier Inc.
0026265X
English
Review

author Emmanuel Ibukun A.; Yahaya N.; Husaini Mohamed A.; Semail N.-F.; Abd Hamid M.A.; Nadhirah Mohamad Zain N.; Anuar Kamaruddin M.; Hong Loh S.; Kamaruzaman S.
spellingShingle Emmanuel Ibukun A.; Yahaya N.; Husaini Mohamed A.; Semail N.-F.; Abd Hamid M.A.; Nadhirah Mohamad Zain N.; Anuar Kamaruddin M.; Hong Loh S.; Kamaruzaman S.
Recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions
author_facet Emmanuel Ibukun A.; Yahaya N.; Husaini Mohamed A.; Semail N.-F.; Abd Hamid M.A.; Nadhirah Mohamad Zain N.; Anuar Kamaruddin M.; Hong Loh S.; Kamaruzaman S.
author_sort Emmanuel Ibukun A.; Yahaya N.; Husaini Mohamed A.; Semail N.-F.; Abd Hamid M.A.; Nadhirah Mohamad Zain N.; Anuar Kamaruddin M.; Hong Loh S.; Kamaruzaman S.
title Recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions
title_short Recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions
title_full Recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions
title_fullStr Recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions
title_full_unstemmed Recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions
title_sort Recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions
publishDate 2024
container_title Microchemical Journal
container_volume 199
container_issue
doi_str_mv 10.1016/j.microc.2024.110111
url https://www.scopus.com/inward/record.uri?eid=2-s2.0-85184484059&doi=10.1016%2fj.microc.2024.110111&partnerID=40&md5=4955a88ecd5bbafa5917f01555da639e
description Over the years, recent advancements have provided new insights into the functionalisation and synthesis of graphene oxide-based materials for sample preparation applications, utilising deep eutectic solvents (DESs). The demand for efficient, selective, innovative, and simple sample preparation of contaminants and pollutants from various matrices has rapidly focused on dispersive and magnetic solid-phase extraction. This study summarises the use of graphene oxide and reduced graphene materials in DES-based synthesis and functionalisation, along with their physicochemical characteristics and applications in dispersive and magnetic solid-phase extraction. The majority of DESs have demonstrated significant enhancements in the extraction of targeted analytes by increasing the effective surface area for active sites and introducing desired functionalities. Upon reviewing the existing literature, it was observed that DESs were functionalised either during or after the production of graphene materials. The findings highlight that dispersive and magnetic solid-phase extraction, incorporated with DES-functionalised graphene adsorbents, offer superior advantages for routine sample pretreatment of analytes, leading to enhanced analytical performance. © 2024 Elsevier B.V.
publisher Elsevier Inc.
issn 0026265X
language English
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