Advances in dispersive solid-phase extraction techniques for analytical quantification of fluoroquinolone antibiotics

Advances in dispersive solid-phase extraction techniques for analytical quantification of fluoroquinolone antibiotics

Misuse and incorrect fluoroquinolones (FQs) disposal have led to environmental pollution and trace amounts of FQs contamination in food chains. Consequently, the quest for innovative, simple, and improved techniques of FQs analyte pre-treatment in real samples has focused on micro- and macroscale di...

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Published in:Microchemical Journal
Main Author: Syaleyana Md Shukri D.; Yahaya N.; Miskam M.; Yusof R.; Husaini Mohamed A.; Kamaruzaman S.; Nadhirah Mohamad Zain N.; Semail N.-F.
Format: Review
Language:English
Published: Elsevier Inc. 2023
Online Access:https://www.scopus.com/inward/record.uri?eid=2-s2.0-85166772694&doi=10.1016%2fj.microc.2023.109154&partnerID=40&md5=f693bd0a299918c97961134b1381d77a
id 2-s2.0-85166772694
spelling 2-s2.0-85166772694
Syaleyana Md Shukri D.; Yahaya N.; Miskam M.; Yusof R.; Husaini Mohamed A.; Kamaruzaman S.; Nadhirah Mohamad Zain N.; Semail N.-F.
Advances in dispersive solid-phase extraction techniques for analytical quantification of fluoroquinolone antibiotics
2023
Microchemical Journal
193

10.1016/j.microc.2023.109154
https://www.scopus.com/inward/record.uri?eid=2-s2.0-85166772694&doi=10.1016%2fj.microc.2023.109154&partnerID=40&md5=f693bd0a299918c97961134b1381d77a
Misuse and incorrect fluoroquinolones (FQs) disposal have led to environmental pollution and trace amounts of FQs contamination in food chains. Consequently, the quest for innovative, simple, and improved techniques of FQs analyte pre-treatment in real samples has focused on micro- and macroscale dispersive solid-phase extraction (DSPE). Recent studies have reported implementing DSPE-based techniques as a sample preparation step to determine FQs in various sample matrices. The present study summarises current FQs detection methods with various chromatographic and DSPE-based combinations. Furthermore, the merits and the analytical figures of DSPE performance when employed for actual samples were discussed. This study also comprehensively evaluated corresponding challenges, opportunities, and the potential of DSPE in detecting trace levels of FQs. The findings demonstrated that the DSPE-based technique provided undeniable advantages for routine sample pre-treatment of FQs and enhanced analytical performance. © 2023 Elsevier B.V.
Elsevier Inc.
0026265X
English
Review
author Syaleyana Md Shukri D.; Yahaya N.; Miskam M.; Yusof R.; Husaini Mohamed A.; Kamaruzaman S.; Nadhirah Mohamad Zain N.; Semail N.-F.
spellingShingle Syaleyana Md Shukri D.; Yahaya N.; Miskam M.; Yusof R.; Husaini Mohamed A.; Kamaruzaman S.; Nadhirah Mohamad Zain N.; Semail N.-F.
Advances in dispersive solid-phase extraction techniques for analytical quantification of fluoroquinolone antibiotics
author_facet Syaleyana Md Shukri D.; Yahaya N.; Miskam M.; Yusof R.; Husaini Mohamed A.; Kamaruzaman S.; Nadhirah Mohamad Zain N.; Semail N.-F.
author_sort Syaleyana Md Shukri D.; Yahaya N.; Miskam M.; Yusof R.; Husaini Mohamed A.; Kamaruzaman S.; Nadhirah Mohamad Zain N.; Semail N.-F.
title Advances in dispersive solid-phase extraction techniques for analytical quantification of fluoroquinolone antibiotics
title_short Advances in dispersive solid-phase extraction techniques for analytical quantification of fluoroquinolone antibiotics
title_full Advances in dispersive solid-phase extraction techniques for analytical quantification of fluoroquinolone antibiotics
title_fullStr Advances in dispersive solid-phase extraction techniques for analytical quantification of fluoroquinolone antibiotics
title_full_unstemmed Advances in dispersive solid-phase extraction techniques for analytical quantification of fluoroquinolone antibiotics
title_sort Advances in dispersive solid-phase extraction techniques for analytical quantification of fluoroquinolone antibiotics
publishDate 2023
container_title Microchemical Journal
container_volume 193
container_issue
doi_str_mv 10.1016/j.microc.2023.109154
url https://www.scopus.com/inward/record.uri?eid=2-s2.0-85166772694&doi=10.1016%2fj.microc.2023.109154&partnerID=40&md5=f693bd0a299918c97961134b1381d77a
description Misuse and incorrect fluoroquinolones (FQs) disposal have led to environmental pollution and trace amounts of FQs contamination in food chains. Consequently, the quest for innovative, simple, and improved techniques of FQs analyte pre-treatment in real samples has focused on micro- and macroscale dispersive solid-phase extraction (DSPE). Recent studies have reported implementing DSPE-based techniques as a sample preparation step to determine FQs in various sample matrices. The present study summarises current FQs detection methods with various chromatographic and DSPE-based combinations. Furthermore, the merits and the analytical figures of DSPE performance when employed for actual samples were discussed. This study also comprehensively evaluated corresponding challenges, opportunities, and the potential of DSPE in detecting trace levels of FQs. The findings demonstrated that the DSPE-based technique provided undeniable advantages for routine sample pre-treatment of FQs and enhanced analytical performance. © 2023 Elsevier B.V.
publisher Elsevier Inc.
issn 0026265X
language English
format Review
accesstype
record_format scopus
collection Scopus
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