Sampling and Sample Preparation Techniques for the Analysis of Organophosphorus Pesticides in Soil Matrices
Despite organophosphorus pesticides (OPPs) benefits in controlling vector-borne diseases and noxious insects, the bioaccumulation and persistence in the soil system may metamorphose into new substances which could pose a serious threat to the ecosystems and human health. The generally low levels of...
Published in: | Critical Reviews in Analytical Chemistry |
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Taylor and Francis Ltd.
2023
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2-s2.0-85118171059 Mohamed A.H.; Noorhisham N.A.; Yahaya N.; Mohamad S.; Kamaruzzaman S.; Osman H.; Aboul-Enein H.Y. Sampling and Sample Preparation Techniques for the Analysis of Organophosphorus Pesticides in Soil Matrices 2023 Critical Reviews in Analytical Chemistry 53 4 10.1080/10408347.2021.1992262 https://www.scopus.com/inward/record.uri?eid=2-s2.0-85118171059&doi=10.1080%2f10408347.2021.1992262&partnerID=40&md5=90276e7a28d1843c88567625528e8f94 Despite organophosphorus pesticides (OPPs) benefits in controlling vector-borne diseases and noxious insects, the bioaccumulation and persistence in the soil system may metamorphose into new substances which could pose a serious threat to the ecosystems and human health. The generally low levels of OPPs residues and often the complexity of the soil matrix are the issues that researcher must deal with. Thus, it is essential to isolate and preconcentrate the OPPs from the matrix to reduce interference effects to obtain a reliable detection. Researchers have reported sample preparation techniques as a promising approach to improve analytical measurement of merits including recovery, precision, linearity, limit of detection, and limit of quantification. Under the selected conditions, limits of detection range between 0.001 and 143 ng/mL, and extraction recovery range between 5 and 154% were obtained. This review evaluates the challenges and opportunities, emphasizes the prospects of sampling techniques and various (micro)extraction coupled with chromatographic methods in different soil samples. Based on the finding, the extraction efficiency depended largely on the interaction between OPPs and extraction media. The fate, migration, toxicity impact, sampling procedure, and storage which influenced the sample preparation were comprehensively discussed. © 2021 Taylor & Francis Group, LLC. Taylor and Francis Ltd. 10408347 English Review |
author |
Mohamed A.H.; Noorhisham N.A.; Yahaya N.; Mohamad S.; Kamaruzzaman S.; Osman H.; Aboul-Enein H.Y. |
spellingShingle |
Mohamed A.H.; Noorhisham N.A.; Yahaya N.; Mohamad S.; Kamaruzzaman S.; Osman H.; Aboul-Enein H.Y. Sampling and Sample Preparation Techniques for the Analysis of Organophosphorus Pesticides in Soil Matrices |
author_facet |
Mohamed A.H.; Noorhisham N.A.; Yahaya N.; Mohamad S.; Kamaruzzaman S.; Osman H.; Aboul-Enein H.Y. |
author_sort |
Mohamed A.H.; Noorhisham N.A.; Yahaya N.; Mohamad S.; Kamaruzzaman S.; Osman H.; Aboul-Enein H.Y. |
title |
Sampling and Sample Preparation Techniques for the Analysis of Organophosphorus Pesticides in Soil Matrices |
title_short |
Sampling and Sample Preparation Techniques for the Analysis of Organophosphorus Pesticides in Soil Matrices |
title_full |
Sampling and Sample Preparation Techniques for the Analysis of Organophosphorus Pesticides in Soil Matrices |
title_fullStr |
Sampling and Sample Preparation Techniques for the Analysis of Organophosphorus Pesticides in Soil Matrices |
title_full_unstemmed |
Sampling and Sample Preparation Techniques for the Analysis of Organophosphorus Pesticides in Soil Matrices |
title_sort |
Sampling and Sample Preparation Techniques for the Analysis of Organophosphorus Pesticides in Soil Matrices |
publishDate |
2023 |
container_title |
Critical Reviews in Analytical Chemistry |
container_volume |
53 |
container_issue |
4 |
doi_str_mv |
10.1080/10408347.2021.1992262 |
url |
https://www.scopus.com/inward/record.uri?eid=2-s2.0-85118171059&doi=10.1080%2f10408347.2021.1992262&partnerID=40&md5=90276e7a28d1843c88567625528e8f94 |
description |
Despite organophosphorus pesticides (OPPs) benefits in controlling vector-borne diseases and noxious insects, the bioaccumulation and persistence in the soil system may metamorphose into new substances which could pose a serious threat to the ecosystems and human health. The generally low levels of OPPs residues and often the complexity of the soil matrix are the issues that researcher must deal with. Thus, it is essential to isolate and preconcentrate the OPPs from the matrix to reduce interference effects to obtain a reliable detection. Researchers have reported sample preparation techniques as a promising approach to improve analytical measurement of merits including recovery, precision, linearity, limit of detection, and limit of quantification. Under the selected conditions, limits of detection range between 0.001 and 143 ng/mL, and extraction recovery range between 5 and 154% were obtained. This review evaluates the challenges and opportunities, emphasizes the prospects of sampling techniques and various (micro)extraction coupled with chromatographic methods in different soil samples. Based on the finding, the extraction efficiency depended largely on the interaction between OPPs and extraction media. The fate, migration, toxicity impact, sampling procedure, and storage which influenced the sample preparation were comprehensively discussed. © 2021 Taylor & Francis Group, LLC. |
publisher |
Taylor and Francis Ltd. |
issn |
10408347 |
language |
English |
format |
Review |
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record_format |
scopus |
collection |
Scopus |
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1809677781544468480 |