Analysis of GC-FID and GC-MS Microwave-Assisted Hydrodistillation Extraction (MAHD) of Agarwood Chips

Abstract: This paper presents an analysis of Gas Chromatography – Flame Ionization Detector (GC-FID) and Gas Chromatography – Mass Spectrometry (GC-MS) microwave-assisted hydrodistillation extraction (MAHD) of agarwood chips. The work involves of agarwood chips sample preparation starting from dryin...

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Published in:International Journal of Integrated Engineering
Main Author: Sarih N.M.; Ismail N.; Akhtar N.; Tajuddin S.N.
Format: Article
Language:English
Published: Penerbit UTHM 2021
Online Access:https://www.scopus.com/inward/record.uri?eid=2-s2.0-85115817139&doi=10.30880%2fijie.2021.13.06.017&partnerID=40&md5=2fc93b41b6af18607d4bb1b320cfee2c
id 2-s2.0-85115817139
spelling 2-s2.0-85115817139
Sarih N.M.; Ismail N.; Akhtar N.; Tajuddin S.N.
Analysis of GC-FID and GC-MS Microwave-Assisted Hydrodistillation Extraction (MAHD) of Agarwood Chips
2021
International Journal of Integrated Engineering
13
6
10.30880/ijie.2021.13.06.017
https://www.scopus.com/inward/record.uri?eid=2-s2.0-85115817139&doi=10.30880%2fijie.2021.13.06.017&partnerID=40&md5=2fc93b41b6af18607d4bb1b320cfee2c
Abstract: This paper presents an analysis of Gas Chromatography – Flame Ionization Detector (GC-FID) and Gas Chromatography – Mass Spectrometry (GC-MS) microwave-assisted hydrodistillation extraction (MAHD) of agarwood chips. The work involves of agarwood chips sample preparation starting from drying to soaking process, extraction method using MAHD and compound analysis using GC-FID and GC-MS for compounds identification. During the extraction time, four hours were varied; 2-hours, 3-hours, 4-hours The result showed that the agarwood chips in this study, extracted by MAHD are made up of three major groups; oxygenated sesquiterpenes, monoterpene hydrocarbons, and sesquiterpene hydrocarbons. Not limited to that, the study also adds to the understanding of the variation of the chemical compounds in agarwood especially those contributed to the fragrance of its oil as well as together with different hours of extraction time where n-hexadecanoic acid appeared as the compound to have the high peak of relative peak area (%) at all (5, 4, 3 and 2) time of extractions. © 2021. UTHM Publisher. All rights reserved.
Penerbit UTHM
2229838X
English
Article
All Open Access; Hybrid Gold Open Access
author Sarih N.M.; Ismail N.; Akhtar N.; Tajuddin S.N.
spellingShingle Sarih N.M.; Ismail N.; Akhtar N.; Tajuddin S.N.
Analysis of GC-FID and GC-MS Microwave-Assisted Hydrodistillation Extraction (MAHD) of Agarwood Chips
author_facet Sarih N.M.; Ismail N.; Akhtar N.; Tajuddin S.N.
author_sort Sarih N.M.; Ismail N.; Akhtar N.; Tajuddin S.N.
title Analysis of GC-FID and GC-MS Microwave-Assisted Hydrodistillation Extraction (MAHD) of Agarwood Chips
title_short Analysis of GC-FID and GC-MS Microwave-Assisted Hydrodistillation Extraction (MAHD) of Agarwood Chips
title_full Analysis of GC-FID and GC-MS Microwave-Assisted Hydrodistillation Extraction (MAHD) of Agarwood Chips
title_fullStr Analysis of GC-FID and GC-MS Microwave-Assisted Hydrodistillation Extraction (MAHD) of Agarwood Chips
title_full_unstemmed Analysis of GC-FID and GC-MS Microwave-Assisted Hydrodistillation Extraction (MAHD) of Agarwood Chips
title_sort Analysis of GC-FID and GC-MS Microwave-Assisted Hydrodistillation Extraction (MAHD) of Agarwood Chips
publishDate 2021
container_title International Journal of Integrated Engineering
container_volume 13
container_issue 6
doi_str_mv 10.30880/ijie.2021.13.06.017
url https://www.scopus.com/inward/record.uri?eid=2-s2.0-85115817139&doi=10.30880%2fijie.2021.13.06.017&partnerID=40&md5=2fc93b41b6af18607d4bb1b320cfee2c
description Abstract: This paper presents an analysis of Gas Chromatography – Flame Ionization Detector (GC-FID) and Gas Chromatography – Mass Spectrometry (GC-MS) microwave-assisted hydrodistillation extraction (MAHD) of agarwood chips. The work involves of agarwood chips sample preparation starting from drying to soaking process, extraction method using MAHD and compound analysis using GC-FID and GC-MS for compounds identification. During the extraction time, four hours were varied; 2-hours, 3-hours, 4-hours The result showed that the agarwood chips in this study, extracted by MAHD are made up of three major groups; oxygenated sesquiterpenes, monoterpene hydrocarbons, and sesquiterpene hydrocarbons. Not limited to that, the study also adds to the understanding of the variation of the chemical compounds in agarwood especially those contributed to the fragrance of its oil as well as together with different hours of extraction time where n-hexadecanoic acid appeared as the compound to have the high peak of relative peak area (%) at all (5, 4, 3 and 2) time of extractions. © 2021. UTHM Publisher. All rights reserved.
publisher Penerbit UTHM
issn 2229838X
language English
format Article
accesstype All Open Access; Hybrid Gold Open Access
record_format scopus
collection Scopus
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