Crystal structure of bis(2-methoxy-6-((Z)-(p-tolylimino)methyl)phenoxy)palladium
The structure of bis(2-methoxy-6-((Z)-(p-tolylimino)methyl)phenoxy)palladium crystallized in a monoclinic system and was characterized thus: P21/c, a = 13.0221(14), b = 11.6615(13), c = 8.4898(9)Å, β = 97.327(4)°, Z = 2, V = 1278.7(2)Å3. The crystal structure was solved by direct methods and refined...
| Published in: | X-ray Structure Analysis Online |
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| Format: | Article |
| Language: | English |
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Japan Society for Analytical Chemistry
2019
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| Online Access: | https://www.scopus.com/inward/record.uri?eid=2-s2.0-85067995139&doi=10.2116%2fxraystruct.35.25&partnerID=40&md5=af883d0889e577721402ed1173f7b1ca |
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2-s2.0-85067995139 |
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2-s2.0-85067995139 Kassim K.; Kahar M.A.M.; Yamin B.M.; Manan M.A.F.A.; Yusof M.S.M. Crystal structure of bis(2-methoxy-6-((Z)-(p-tolylimino)methyl)phenoxy)palladium 2019 X-ray Structure Analysis Online 35 4 10.2116/xraystruct.35.25 https://www.scopus.com/inward/record.uri?eid=2-s2.0-85067995139&doi=10.2116%2fxraystruct.35.25&partnerID=40&md5=af883d0889e577721402ed1173f7b1ca The structure of bis(2-methoxy-6-((Z)-(p-tolylimino)methyl)phenoxy)palladium crystallized in a monoclinic system and was characterized thus: P21/c, a = 13.0221(14), b = 11.6615(13), c = 8.4898(9)Å, β = 97.327(4)°, Z = 2, V = 1278.7(2)Å3. The crystal structure was solved by direct methods and refined by full-matrix least-squares on F2 to final values of R1 = 0.0349 [I > 2σ(I)] and wR2 = 0.0824. The molecules have two-fold symmetry about the centre Pd1 atom. Two ligands were coordinated to the Pd1 atom via oxygen and nitrogen atoms in a bidentate manner to form a square-planar geometrical structure. © 2019, The Japan Society for Analytical Chemistry. Japan Society for Analytical Chemistry 18833578 English Article All Open Access; Gold Open Access |
| author |
Kassim K.; Kahar M.A.M.; Yamin B.M.; Manan M.A.F.A.; Yusof M.S.M. |
| spellingShingle |
Kassim K.; Kahar M.A.M.; Yamin B.M.; Manan M.A.F.A.; Yusof M.S.M. Crystal structure of bis(2-methoxy-6-((Z)-(p-tolylimino)methyl)phenoxy)palladium |
| author_facet |
Kassim K.; Kahar M.A.M.; Yamin B.M.; Manan M.A.F.A.; Yusof M.S.M. |
| author_sort |
Kassim K.; Kahar M.A.M.; Yamin B.M.; Manan M.A.F.A.; Yusof M.S.M. |
| title |
Crystal structure of bis(2-methoxy-6-((Z)-(p-tolylimino)methyl)phenoxy)palladium |
| title_short |
Crystal structure of bis(2-methoxy-6-((Z)-(p-tolylimino)methyl)phenoxy)palladium |
| title_full |
Crystal structure of bis(2-methoxy-6-((Z)-(p-tolylimino)methyl)phenoxy)palladium |
| title_fullStr |
Crystal structure of bis(2-methoxy-6-((Z)-(p-tolylimino)methyl)phenoxy)palladium |
| title_full_unstemmed |
Crystal structure of bis(2-methoxy-6-((Z)-(p-tolylimino)methyl)phenoxy)palladium |
| title_sort |
Crystal structure of bis(2-methoxy-6-((Z)-(p-tolylimino)methyl)phenoxy)palladium |
| publishDate |
2019 |
| container_title |
X-ray Structure Analysis Online |
| container_volume |
35 |
| container_issue |
4 |
| doi_str_mv |
10.2116/xraystruct.35.25 |
| url |
https://www.scopus.com/inward/record.uri?eid=2-s2.0-85067995139&doi=10.2116%2fxraystruct.35.25&partnerID=40&md5=af883d0889e577721402ed1173f7b1ca |
| description |
The structure of bis(2-methoxy-6-((Z)-(p-tolylimino)methyl)phenoxy)palladium crystallized in a monoclinic system and was characterized thus: P21/c, a = 13.0221(14), b = 11.6615(13), c = 8.4898(9)Å, β = 97.327(4)°, Z = 2, V = 1278.7(2)Å3. The crystal structure was solved by direct methods and refined by full-matrix least-squares on F2 to final values of R1 = 0.0349 [I > 2σ(I)] and wR2 = 0.0824. The molecules have two-fold symmetry about the centre Pd1 atom. Two ligands were coordinated to the Pd1 atom via oxygen and nitrogen atoms in a bidentate manner to form a square-planar geometrical structure. © 2019, The Japan Society for Analytical Chemistry. |
| publisher |
Japan Society for Analytical Chemistry |
| issn |
18833578 |
| language |
English |
| format |
Article |
| accesstype |
All Open Access; Gold Open Access |
| record_format |
scopus |
| collection |
Scopus |
| _version_ |
1809677906049236992 |