Phytochemical study on the stem bark of Mallotus leucodermis Hook F.; [Kajian fitokimia ke atas kulit ranting Mallotus leucodermis Hook F.]

Phytochemical study on the stem bark of Mallotus leucodermis Hook F.; [Kajian fitokimia ke atas kulit ranting Mallotus leucodermis Hook F.]

The stem barks of Mallotus leucodermis Hook F. (Euphorbiaceae) was studied for its chemical constituents. The air dried and pulverized of stem bark of M. leucodermis (1.3 kg) was extracted successively with acetone for three days at room temperature yielding 66.0 g of crude extract. The crude extrac...

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Published in:Malaysian Journal of Analytical Sciences
Main Author: Mohd Yusoff A.S.; Ahmat N.; Naz H.
Format: Article
Language:English
Published: Malaysian Society of Analytical Sciences 2016
Online Access:https://www.scopus.com/inward/record.uri?eid=2-s2.0-84977119393&doi=10.17576%2fmjas-2016-2003-12&partnerID=40&md5=e37c76a3700ce9425491d1d1ff3aa0d0
id 2-s2.0-84977119393
spelling 2-s2.0-84977119393
Mohd Yusoff A.S.; Ahmat N.; Naz H.
Phytochemical study on the stem bark of Mallotus leucodermis Hook F.; [Kajian fitokimia ke atas kulit ranting Mallotus leucodermis Hook F.]
2016
Malaysian Journal of Analytical Sciences
20
3
10.17576/mjas-2016-2003-12
https://www.scopus.com/inward/record.uri?eid=2-s2.0-84977119393&doi=10.17576%2fmjas-2016-2003-12&partnerID=40&md5=e37c76a3700ce9425491d1d1ff3aa0d0
The stem barks of Mallotus leucodermis Hook F. (Euphorbiaceae) was studied for its chemical constituents. The air dried and pulverized of stem bark of M. leucodermis (1.3 kg) was extracted successively with acetone for three days at room temperature yielding 66.0 g of crude extract. The crude extract was fractionated using vacuum liquid chromatography (VLC) to afford six fractions. Fraction 6 was further washed and recrystallized to afford bergenin (1). Fraction 3 was subjected to multiple purification using radial chromatography (CHCl3: acetone) with different ratio 9:1, 8:2, 6:4 and 5:5 to yield a flavonoid compound, epicatechin (2). These compounds were elucidated based on spectroscopic analysis (Ultra Violate, Infra-Red, Mass Spectrometry and Nuclear Magnetic Resonance) as well as comparison with literatures. © 2016, Malaysian Society of Analytical Sciences. All rights reserved.
Malaysian Society of Analytical Sciences
13942506
English
Article
All Open Access; Gold Open Access
author Mohd Yusoff A.S.; Ahmat N.; Naz H.
spellingShingle Mohd Yusoff A.S.; Ahmat N.; Naz H.
Phytochemical study on the stem bark of Mallotus leucodermis Hook F.; [Kajian fitokimia ke atas kulit ranting Mallotus leucodermis Hook F.]
author_facet Mohd Yusoff A.S.; Ahmat N.; Naz H.
author_sort Mohd Yusoff A.S.; Ahmat N.; Naz H.
title Phytochemical study on the stem bark of Mallotus leucodermis Hook F.; [Kajian fitokimia ke atas kulit ranting Mallotus leucodermis Hook F.]
title_short Phytochemical study on the stem bark of Mallotus leucodermis Hook F.; [Kajian fitokimia ke atas kulit ranting Mallotus leucodermis Hook F.]
title_full Phytochemical study on the stem bark of Mallotus leucodermis Hook F.; [Kajian fitokimia ke atas kulit ranting Mallotus leucodermis Hook F.]
title_fullStr Phytochemical study on the stem bark of Mallotus leucodermis Hook F.; [Kajian fitokimia ke atas kulit ranting Mallotus leucodermis Hook F.]
title_full_unstemmed Phytochemical study on the stem bark of Mallotus leucodermis Hook F.; [Kajian fitokimia ke atas kulit ranting Mallotus leucodermis Hook F.]
title_sort Phytochemical study on the stem bark of Mallotus leucodermis Hook F.; [Kajian fitokimia ke atas kulit ranting Mallotus leucodermis Hook F.]
publishDate 2016
container_title Malaysian Journal of Analytical Sciences
container_volume 20
container_issue 3
doi_str_mv 10.17576/mjas-2016-2003-12
url https://www.scopus.com/inward/record.uri?eid=2-s2.0-84977119393&doi=10.17576%2fmjas-2016-2003-12&partnerID=40&md5=e37c76a3700ce9425491d1d1ff3aa0d0
description The stem barks of Mallotus leucodermis Hook F. (Euphorbiaceae) was studied for its chemical constituents. The air dried and pulverized of stem bark of M. leucodermis (1.3 kg) was extracted successively with acetone for three days at room temperature yielding 66.0 g of crude extract. The crude extract was fractionated using vacuum liquid chromatography (VLC) to afford six fractions. Fraction 6 was further washed and recrystallized to afford bergenin (1). Fraction 3 was subjected to multiple purification using radial chromatography (CHCl3: acetone) with different ratio 9:1, 8:2, 6:4 and 5:5 to yield a flavonoid compound, epicatechin (2). These compounds were elucidated based on spectroscopic analysis (Ultra Violate, Infra-Red, Mass Spectrometry and Nuclear Magnetic Resonance) as well as comparison with literatures. © 2016, Malaysian Society of Analytical Sciences. All rights reserved.
publisher Malaysian Society of Analytical Sciences
issn 13942506
language English
format Article
accesstype All Open Access; Gold Open Access
record_format scopus
collection Scopus
_version_ 1809677910298066944

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