Solvothermal synthesized of TiO2 microspheres and their characterization
In this paper, we have successfully synthesized TiO2 microsperes by solvothermal method using titanium (IV) isopropoxide as titanium source and ethanol as a solvent. The solution was thermally treated at relatively low temperature of 150 °C for 3 hours. The as-prepared and annealed of TiO2 microsphe...
| Published in: | Advanced Materials Research |
|---|---|
| Main Author: | |
| Format: | Conference paper |
| Language: | English |
| Published: |
2012
|
| Online Access: | https://www.scopus.com/inward/record.uri?eid=2-s2.0-84869383086&doi=10.4028%2fwww.scientific.net%2fAMR.576.345&partnerID=40&md5=eed19d597516aef8e49dc9e9f62b67c3 |
| Summary: | In this paper, we have successfully synthesized TiO2 microsperes by solvothermal method using titanium (IV) isopropoxide as titanium source and ethanol as a solvent. The solution was thermally treated at relatively low temperature of 150 °C for 3 hours. The as-prepared and annealed of TiO2 microsphere were characterized using FESEM, XRD and Raman spectroscopy. The diameter of the microspheres was 1-6 μm. The X-ray diffraction and Raman spectroscopy studies show that the microspheres has anatase phase. © (2012) Trans Tech Publications, Switzerland. |
|---|---|
| ISSN: | 10226680 |
| DOI: | 10.4028/www.scientific.net/AMR.576.345 |